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Mesoporous silica of SBA-15 sort was modified for the primary time with 3-(trihydroxysiyl)-1-propanesulfonic acid (TPS) by submit-synthesis modification involving microwave or standard heating with the intention to generate the Brønsted acidic centers on the fabric surface. The samples structure and composition have been examined by low temperature N2 adsorption/desorption, XRD, HRTEM, elemental and thermal analyses. The floor properties were evaluated by esterification of acetic acid with n-hexanol used as the take a look at reaction. A a lot higher effectivity of TPS species incorporation was reached with the appliance of microwave radiation for 1 h than typical modification for 24 h. It was discovered that the construction of mesoporous help was preserved after modification utilizing each strategies utilized in this research. Materials obtained with the use of microwave radiation showed a superior catalytic activity and high stability. Engaged on a manuscript? The structure of those solids is characterized by relatively massive floor area, e.g. One thousand m2 g−1, and the presence of hexagonal channels common in measurement.

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